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NMR Basic Principles and Progress

Solid-State NMR III Organic Matter

Organic Matter

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About this book

Solid-State NMR is a branch of Nuclear Magnetic Resonance which is presently experiencing a phase of strongly increasing popularity. The most striking evidence is the large number of contributions from Solid-State Resonance atNMR meetings, approaching that ofliquid­ state resonance. Important progress can be observed in three areas: Methodological developments, applications to inorganic matter, and applications to organic matter. These developments are intented to be captured in three volumes in this series, each of them being devoted to more or less one of these areas. The present volume on Solid-State NMR III is devoted mainly to organic matter. The recent developments of deuteron NMR and their applications are reviewed in the first chapter. Crosspolarization, MAS, and dynamic angle spinning are being explored for enhancement of information and sensitivity. In addition to the analysis of classical relaxation times and modern 2D spectra, detailed dynamic information becomes accessible from investigations of the relaxation time anisotropies. The second chapter examines cross-polarization in static and rotating solids under conditions of spin diffusion and thermal motion. The underlying dipole-dipole interaction is further exploited by the techniques described in the third chapter for studies of polymer-polymer miscibility. Short­ range techniques are discriminated from long-range techniques based on spin diffusion. The use ofthese techniques is illustrated by a case study ofPMMAJPVF blends. The last chapter addresses novel z methods and applications of two-dimensional exchange NMR for investigations of relative molecular orientations, polymer morphology, molecular dynamics, and macroscopic molecular order.

Table of contents (4 chapters)

Table of contents (4 chapters)
  • 2H-NMR Spectroscopy of Solids and Liquid Crystals

    Pages 1-67

    Hoatson, G. L. (et al.)

  • Cross-Polarization, Relaxation Times and Spin-Diffusion in Rotating Solids

    Pages 69-125

    Michel, D. (et al.)

  • Solid State NMR Techniques for the Study of Polymer-Polymer Miscibility

    Pages 127-162

    Veeman, W. S. (et al.)

  • Two-Dimensional Exchange NMR Spectroscopy in Polymer Research

    Pages 163-209

    Beckham, H. W. (et al.)

Buy this book

eBook $169.00
price for USA in USD (gross)
  • ISBN 978-3-642-61223-7
  • Digitally watermarked, DRM-free
  • Included format: PDF
  • ebooks can be used on all reading devices
  • Immediate eBook download after purchase
Softcover $219.99
price for USA in USD
  • ISBN 978-3-642-64751-2
  • Free shipping for individuals worldwide
  • Usually dispatched within 3 to 5 business days.
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Bibliographic Information

Bibliographic Information
Book Title
Solid-State NMR III Organic Matter
Book Subtitle
Organic Matter
Series Title
NMR Basic Principles and Progress
Series Volume
32
Copyright
1994
Publisher
Springer-Verlag Berlin Heidelberg
Copyright Holder
Springer-Verlag Berlin Heidelberg
eBook ISBN
978-3-642-61223-7
DOI
10.1007/978-3-642-61223-7
Softcover ISBN
978-3-642-64751-2
Series ISSN
0170-5989
Edition Number
1
Number of Pages
X, 213
Topics