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  • © 2023

Springer Handbook of Advanced Catalyst Characterization

  • Presents expert knowledge in all characterization techniques for catalytic materials at the atomic and molecular levels
  • Details information on the characterization of bulk and surface of solid catalytic materials
  • Provides insight on emerging methodologies and advanced in situ and operando spectroscopy characterization methods

Part of the book series: Springer Handbooks (SHB)

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Table of contents (48 chapters)

  1. Front Matter

    Pages i-xxix
  2. Vibrational Spectroscopy

    1. Front Matter

      Pages 1-1
    2. Infrared (IR) Spectroscopy

      • Guido Busca
      Pages 3-32
    3. Case Studies: Infrared (IR) Spectroscopy

      • Chiara Negri, Michele Carosso, Eleonora Vottero, Elena Groppo, Silvia Bordiga
      Pages 33-52
    4. Reflection Absorption Infrared Spectroscopy

      • Ravi Ranjan, Michael Trenary
      Pages 53-73
    5. Raman Spectroscopy

      • Jisue Moon, Meijun Li, Anibal J. Ramirez-Cuesta, Zili Wu
      Pages 75-110
    6. Case Studies: Raman Spectroscopy

      • Ragamaye Tigiripalli, Vishal Agarwal, Goutam Deo
      Pages 111-129
    7. Ultraviolet (UV) Raman Spectroscopy

      • Peter C. Stair
      Pages 131-149
    8. Surface Enhanced Raman Spectroscopy (SERS)

      • Ramón A. Alvarez-Puebla
      Pages 151-168
    9. Nanoscale Raman Spectroscopy

      • Tanja Deckert-Gaudig, Marie Richard-Lacroix, Volker Deckert
      Pages 169-188
    10. Operando Electrochemical Raman Spectroscopy

      • Wolfgang Schuhmann, Denis Öhl, Dulce M. Morales
      Pages 189-211
    11. Sum Frequency Generation (SFG) Spectroscopy

      • Verena Pramhaas, Günther Rupprechter
      Pages 213-233
  3. Electron and Photoelectron Spectroscopy

    1. Front Matter

      Pages 235-235
    2. Ultraviolet-Visible (UV-Vis) Spectroscopy

      • Charlotte Vogt, Caterina Suzanna Wondergem, Bert M. Weckhuysen
      Pages 237-264
    3. Case Studies: Ultraviolet-Visible (UV-Vis) Spectroscopy

      • Zixu Yang, Minghui Zhu
      Pages 265-283
    4. Fluorescence Microscopy

      • Xianwen Mao, Rong Ye, Peng Chen
      Pages 285-294
    5. Photoluminescence (PL) Spectroscopy

      • Qinghe Li, Masakazu Anpo, Jinmao You, Tingjiang Yan, Xinchen Wang
      Pages 295-321
    6. Case Studies: Photoluminescence (PL) Spectroscopy

      • Lorenzo Mino, Masaya Matsuoka, Gianmario Martra
      Pages 323-336
    7. Near Ambient Pressure (NAP) X-Ray Photoelectron Spectroscopy (XPS)

      • Zongyuan Liu, Sanjaya Senanayake, José A. Rodriguez
      Pages 337-345

About this book

Co-edited by world-renowned scientists in the field of catalysis, this book contains the cutting-edge in situ and operando spectroscopy characterization techniques operating under reaction conditions to determine a materials’ bulk, surface, and solution complex and their applications in the field of catalysis with emphasis on solid catalysts in powder form since such catalyst are relevant for industrial applications. The handbook covers from widely-used to cutting-edge techniques. The handbook is written for a broad audience of students and professionals who want to pursue the full capabilities available by the current state-of-the-art in characterization to fully understand how their catalysts really operate and guide the rational design of advanced catalysts.

Individuals involved in catalysis research will be interested in this handbook because it contains a catalogue of cutting-edge methods employed in characterization of catalysts.  These techniques find wide use in applications such as petroleum refining, chemical manufacture, natural gas conversion, pollution control, transportation, power generation, pharmaceuticals and food processing. 

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Editors and Affiliations

  • Operando Molecular Spectroscopy & Catalysis Laboratory, Department of Chemical & Biomolecular Engineering Lehigh University, Bethlehem, USA

    Israel E. Wachs

  • Catalytic Spectroscopy Laboratory, Spectroscopy and Industrial Catalysis, SpeiCat Institute for Catalysis and Petroleum Chemistry, CSIC, Madrid, Spain

    Miguel A. Bañares

About the editors

Israel E. Wachs is G. Whitney Snyder Professor of Chemical and Biomolecular Engineering and Director of the Operando Molecular Spectroscopy and Catalysis Laboratory at Lehigh University, Bethlehem, PA, USA. He has earned wide recognition for his pioneering research into heterogeneous catalysis of mixed oxides for his modern approach to establishing fundamental relationships between surface structure and kinetic activity/selectivity. In 2016, he received AIChE’s top award in chemical reaction engineering, the R. H. Wilhelm Award, sponsored by ExxonMobil Research for seminal contributions toward the development of innovative concepts for molecular chemical reaction engineering of mixed oxide catalyzed reactions by establishing fundamental catalyst molecular structure-activity kinetic relationships. He has also been honored for his work on green chemistry technologies by the U.S. Environmental Protection Agency (EPA). Dr. Wachs received his B.S. from the City College of the CityUniversity of New York and his M.S. and Ph.D. degrees from Stanford University.                      

Miguel A. Bañares is Full Research Professor at the Institute for Catalysis and Petroleum Chemistry, CSIC, in Madrid, Spain. He has been deputy vice president for Scientific-Technical Fields at CSIC, Spanish National Research Council. The Bañares group focuses its research on understanding structure-performance relationships in catalysis combining spectroscopy during catalytic reactions with simultaneous activity measurement (operando methodology, a term that he coined in 2000) for real-time monitoring of catalytic processes, catalyst evolution, and synthesis. He has been awarded the Doctor Honoris Causa degree by the Université de Caen Normandie, France, for his seminal operando spectroscopy work. Dr. Bañares received the B.S. and Ph.D. degrees from Universidad de Salamanca, Spain.

Bibliographic Information

Buy it now

Buying options

eBook USD 299.00
Price excludes VAT (USA)
  • Available as EPUB and PDF
  • Read on any device
  • Instant download
  • Own it forever
Hardcover Book USD 379.99
Price excludes VAT (USA)
  • Durable hardcover edition
  • Dispatched in 3 to 5 business days
  • Free shipping worldwide - see info

Tax calculation will be finalised at checkout

Other ways to access