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Polymer Fractionation

  • Book
  • © 1994

Overview

Authors:
  1. Frieder Francuskiewicz

    1. Forschungsstelle Dr. Kubsch, Laboratorium für Analytik, Radiometrie und Umwelttechnologie GmbH, FARU, Dresden, Germany

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Part of the book series: Springer Lab Manuals (SLM)

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Table of contents (13 chapters)

  1. Front Matter

    Pages I-XVII
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  2. Introduction

    • Frieder Francuskiewicz
    Pages 1-5

  3. The Size of Polymer Molecules — Mean Values and Distributions of the Molecular Weight

    • Frieder Francuskiewicz
    Pages 6-9

  4. Dissolution and Precipitation of Polymers

    • Frieder Francuskiewicz
    Pages 10-18

  5. Basic Principles of Fractionation Procedures

    • Frieder Francuskiewicz
    Pages 19-38

  6. Precipitation Fractionation

    • Frieder Francuskiewicz
    Pages 39-63

  7. Extraction Fractionation

    • Frieder Francuskiewicz
    Pages 64-104

  8. Gradient-Elution Fractionation

    • Frieder Francuskiewicz
    Pages 105-120

  9. Baker-Williams Fractionation

    • Frieder Francuskiewicz
    Pages 121-130

  10. Trouble Shooting and Large-Scale Techniques in Column Fractionations

    • Frieder Francuskiewicz
    Pages 131-136

  11. Temperature Rising Elution Fractionation

    • Frieder Francuskiewicz
    Pages 137-144

  12. Partition Fractionation

    • Frieder Francuskiewicz
    Pages 145-176

  13. Cross Fractionation

    • Frieder Francuskiewicz
    Pages 177-183

  14. Outlook

    • Frieder Francuskiewicz
    Pages 184-185

  15. Back Matter

    Pages 187-217
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Keywords

About this book

Fractionation of polymers via solubility has been a well known method in polymer characterization for a long time. The original object of analytical fractionations, the determination of the molecular weight distribution, is nowadays achieved more efficiently and conveniently by chromatographic methods. However, fractionation procedures, which were developed in great diversity, remain up~to-date and essential for obtaining preparative fractions with narrow distributions. Such fractions are wanted increasingly for the investigation of true structure-property relationships which are mostly influ~ enced by distributions of molecular weight or other parameters such as branching or chemical composition. Literature on the field of polymer fractionation is extensive and several reviews exist. However, there is a lack of systematically methodical instruc­ tions for carrying-out of diverse fractionation procedures. This volume repre­ sents an attempt to reduce this deficiency and is focussed on practical aspects of fractionation procedures. This laboratory manual is intended for polymer chemists, physicists, and technicians, for students of polymer science, and skilled laboratory assistants, all of whom are not dealing directly with fractionation but are in need of fractions to carry out further investigations.

Authors and Affiliations

  • Forschungsstelle Dr. Kubsch, Laboratorium für Analytik, Radiometrie und Umwelttechnologie GmbH, FARU, Dresden, Germany

    Frieder Francuskiewicz

Bibliographic Information

  • Book Title: Polymer Fractionation

  • Authors: Frieder Francuskiewicz

  • Series Title: Springer Lab Manuals

  • DOI: https://doi.org/10.1007/978-3-642-78704-1

  • Publisher: Springer Berlin, Heidelberg

  • eBook Packages: Springer Book Archive

  • Copyright Information: Springer-Verlag Berlin Heidelberg 1994

  • Hardcover ISBN: 978-3-540-57539-9Due: 30 August 1994

  • Softcover ISBN: 978-3-642-78706-5Published: 24 December 2012

  • eBook ISBN: 978-3-642-78704-1Published: 09 March 2013

  • Edition Number: 1

  • Number of Pages: XVII, 217

  • Number of Illustrations: 22 b/w illustrations

  • Topics: Industrial Chemistry/Chemical Engineering, Polymer Sciences, Analytical Chemistry

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