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Materials Syntheses

A Practical Guide

  • Book
  • © 2008

Overview

Editors:
  1. Ulrich Schubert

    1. Institute of Materials Chemistry, Vienna University of Technology, Vienna, Austria

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    You can also search for this editor in PubMed   Google Scholar

  2. Nicola Hüsing

    1. Inorganic Chemistry I, Ulm University, Ulm, Germany

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    You can also search for this editor in PubMed   Google Scholar

  3. Richard M. Laine

    1. Departments of Chemistry, and Materials Science and Engineering, University of Michigan, Ann Arbor, USA

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    You can also search for this editor in PubMed   Google Scholar

  • First book on detailed materials synthesis protocols

  • Unambiguous descriptions of hardware, specific synthetic procedures and characterization methods

  • Helpful manual for laboratory courses in materials chemistry

  • Includes supplementary material: sn.pub/extras

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Table of contents (28 chapters)

  1. Front Matter

    Pages I-8
    Download chapter PDF

  2. Controlling Size and Morphology of Zeolite L

    • A. Z. Ruiz, D. Brühwiler, L. -Q. Dieu, G. Calzaferri
    Pages 9-19

  3. Zeolite A and ZK-4

    • C. Leiggener, A. Currao, G. Calzaferri
    Pages 21-28

  4. Mesostructured Silica Thin Films

    • J. Köhler, J. Geserick, N. Hüsing
    Pages 29-38

  5. Organically Modified Monolithic Silica Aerogels

    • N. Hüsing, U. Schubert
    Pages 39-45

  6. Porous Silica Gel by Acid Leaching of Metakaolin

    • C. Belver, M. Á. Vicente
    Pages 47-51

  7. Zirconia-Pillared Clays

    • M. A. Vicente, A. Gil
    Pages 53-58

  8. Montmorillonites with Mixed Aluminum-Lanthanide Oxide Pillars

    • C. Pesquera, C. Blanco, F. González
    Pages 59-63

  9. Birnessite-type Manganese Oxide by Redox Precipitation

    • Q. Feng, Z. -H. Liu, K. Ooi
    Pages 65-70

  10. Templated Carbon from Pyrolysis of Pyrene in Pillared Clay Matrices

    • G. Sandí, K. A. Carrado, R. E. Winans
    Pages 71-76

  11. Fiberous Carbon from Sepiolite Clay and Propylene

    • G. Sandí, K. A. Carrado, R. E. Winans
    Pages 77-82

  12. Aerosol Spray Synthesis of Porous Molybdenum Sulfide Powder

    • S. E. Skrabalak, K. Suslick
    Pages 83-88

  13. Sonochemically Prepared Molybdenum Sulfide

    • A. Ryder, K. Suslick
    Pages 89-94

  14. Doped Manganites

    • J. Spooren, R. I. Walton
    Pages 95-102

  15. Lithium Manganese Oxide Prepared by Flux Methods

    • W. Tang, Q. Feng, X. Yang, R. Chitrakar, K. Ooi
    Pages 103-109

  16. Nanoscale Magnesium Oxide

    • F. Khairallah, A. Glisenti
    Pages 111-115

  17. Nanostructured Pt-doped Tin Oxide Films

    • R. Scotti, C. Canevali, M. Mattoni, F. Morazzoni, L. Armelao, D. Barreca
    Pages 117-126

  18. Organically Functionalized Silica Nanoparticles

    • G. Kickelbick, D. Holzinger, S. Ivanovici
    Pages 127-133

  19. Copper Nanoparticles in Silica

    • U. Schubert, C. Lembacher, G. Trimmel
    Pages 135-141

  20. Copper Nanocrystals

    • S. D. Bunge, T. J. Boyle
    Pages 143-148
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Keywords

About this book

Materials syntheses are generally more complex than syntheses of inorganic or organic compounds, and specific characterization methods play a more important role. Materials synthesis protocols often suffer from unclarities, irreproducibility, lack in detail and lack in standards. The need to change this situation is the main motivation for this book. A number of detailed protocols has been collected, ranging from organic polymers to carbonaceous and ceramic materials, from gels to porous and layered materials and from powders and nanoparticles to films. Preparation methods include intercalation and flux methods, sol-gel processing, templating methods for porous materials, sonochemistry or spray pyrolysis.

Each contribution provides detailed and unambiguous description of the hardware, specific characteristics of the procedure, scope of applicability as well as methods that unequivocally identify and characterize the material and allow checking whether the synthesis was successful.

Editors and Affiliations

  • Institute of Materials Chemistry, Vienna University of Technology, Vienna, Austria

    Ulrich Schubert

  • Inorganic Chemistry I, Ulm University, Ulm, Germany

    Nicola Hüsing

  • Departments of Chemistry, and Materials Science and Engineering, University of Michigan, Ann Arbor, USA

    Richard M. Laine

Bibliographic Information

  • Book Title: Materials Syntheses

  • Book Subtitle: A Practical Guide

  • Editors: Ulrich Schubert, Nicola Hüsing, Richard M. Laine

  • DOI: https://doi.org/10.1007/978-3-211-75125-1

  • Publisher: Springer Vienna

  • eBook Packages: Chemistry and Materials Science, Chemistry and Material Science (R0)

  • Copyright Information: Springer-Verlag Vienna 2008

  • Hardcover ISBN: 978-3-211-75124-4Published: 02 July 2008

  • Softcover ISBN: 978-3-211-99912-7Published: 13 October 2010

  • eBook ISBN: 978-3-211-75125-1Published: 23 November 2008

  • Edition Number: 1

  • Number of Pages: VII, 228

  • Topics: Materials Science, general, Inorganic Chemistry, Nanotechnology

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