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Solid State NMR of Polymers

  • Book
  • © 1991

Overview

Editors:
  1. Lon J. Mathias

    1. Department of Polymer Science, University of Southern Mississippi, Hattiesburg, USA

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Table of contents (25 chapters)

  1. Front Matter

    Pages i-ix
    Download chapter PDF

  2. Overviews

    1. Multiple-Pulse 1H and 19F NMR Techniques

      • Cecil Dybowski
      Pages 1-21

    2. Solid-State 2H NMR: Overview with Specific Examples

      • Ronald F. Colletti, Lon J. Mathias
      Pages 23-60

    3. Application of NMR Imaging to Polymers: A Tutorial

      • Jack L. Koenig
      Pages 61-79

  3. 13C CP/MAS Applications

    1. Solid State 13C NMR Studies of the Structures, Conformations, and Dynamics of Semi-Crystalline Polymers

      • A. E. Tonelli, M. A. Gomez, Hajime Tanaka, M. H. Cozine
      Pages 81-105

    2. CP/MAS 13C NMR Analysis of Poly(Arylene Methylene)s

      • Michael L. Froehlich, Martin B. Jones
      Pages 107-116

    3. Radiation Induced Morphological Changes in a Semi-Crystalline Polymer: A 13C NMR Study

      • A. L. Cholli, F. C. Schilling, A. E. Tonelli
      Pages 117-130

    4. 13C NMR Studies of Poly(Vinylidene Fluoride) Blends

      • R. A. Grinsted, J. L. Koenig
      Pages 131-144

    5. Solid State NMR Detection of Molecular-Level Mixing Phenomena in Strongly Interacting Polymer Blends and Phase-Separated Copolymers

      • Laurence A. Belfiore, Thomas J. Lutz, Chihmin Cheng
      Pages 145-165

    6. CP-MAS NMR Spectra of Poly(N-Vinylcarbazole) and of its Charge Transfer Complexes: Preliminary Investigation

      • Almeria Natansohn
      Pages 167-177

    7. 13C NMR of Crosslinked Poly(Methacrylic Anhydride)

      • Diana D. Granger
      Pages 179-200

    8. Application of Solid State 13C NMR Spectroscopy to Sulfur Vulcanized Natural Rubber

      • Jack L. Koenig, Mladen Andreis
      Pages 201-213

    9. A Solid-State 13C NMR Study of Polysiloxane Side-Chain Liquid Crystalline Polymers Containing 2-[4-(2S)-Methyl-Butoxy)-Phenyl]-5-(ω-Alkyl)-1,3,2-Dioxaborinane with Alkyl Being Undecanyl and Octyl

      • B. C. Perry, J. L. Koenig
      Pages 215-232

    10. VT-MAS NMR as a Probe of Molecular Mobility and Local Composition: Solidified Acrylic Dispersions

      • R. Voelkel
      Pages 233-244

  4. Deuterium NMR

    1. Molecular Motion in Crystalline and Mesomorphous Phases of Large Size Cycloalkanes as a Model for Polyethylene

      • Martin Moller, Gerhard Kogler, Dieter Oelfin, Hansotto Drotloff
      Pages 245-259

    2. Solid State NMR Relaxation Study of Liquid Crystal Polymers Employing a Two-Dimensional Technique

      • A. Schleicher, K. Müller, G. Kothe
      Pages 261-270

    3. Dynamics of Surface Bound Polymers and Coupling Agents

      • Frank D. Blum, Robert B. Funchess, Wiriya Meesiri
      Pages 271-281

    4. Solid-State 2H and 13C NMR Study of the Structure of Polyanilines

      • S. Kaplan, E. M. Conwell, A. F. Richter, A. G. MacDiarmid
      Pages 283-294
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About this book

The chapters in this collection are from papers which were presented at a symposium on solid-state NMR of polymers. A two-part program on available NMR techniques applicable to solid polymer analysis was presented at the 3rd Chemical Congress of North American held in Toronto, Ontario, June 5-10,1988. The program was sponsored by the Division of Polymer Chemistry with support provided by the Division, its Industrial Sponsors, and the Donors of the Petroleum Research Fund administered by the American Chemical Society. Co-organizers included Professor Colin Fyfe of the University of British Columbia (Vancouver, Canada), Professor Hans Spiess of the Max Planck Institut fur Polymerforschung (Mainz, West Germany), and myself. The full-day tutorial, which was free to registered attendees, covered the range of topics. The purpose of the tutorial was to provide a basic introduction to the field so that newcomers to its present and future applications could develop sufficient understanding to learn effectively from the subsequent symposium. The first talk attempted to give listeners a feel for the way a novice spectroscopist can learn to use the various NMR techniques to explore his own areas of interest. Simple experiments can provide unique information about solid polymers that can be useful in interpreting synthetic results and in relating solid-state conformation, morphology and molecular motion to physical properties.

Editors and Affiliations

  • Department of Polymer Science, University of Southern Mississippi, Hattiesburg, USA

    Lon J. Mathias

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