Multinuclear NMR

1. Front Matter

   Pages i-xx

   PDF

2. Introduction

   • Joan Mason

   Pages 1-2

3. The Parameters of NMR Spectroscopy

   • Cynthia J. Jameson, Joan Mason

   Pages 3-50

4. The Chemical Shift

   • Cynthia J. Jameson, Joan Mason

   Pages 51-88

5. Spin-Spin Coupling

   • Cynthia J. Jameson

   Pages 89-131

6. Relaxation and Related Time-Dependent Processes

   • Oliver Howarth

   Pages 133-169

7. Hydrogen and Its Isotopes

   • J. W. Akitt

   Pages 171-187

8. The Alkali and Alkaline Earth Metals

   • J. W. Akitt

   Pages 189-220

9. Boron

   • John D. Kennedy

   Pages 221-258

10. Aluminum, Gallium, Indium, and Thallium

    • J. W. Akitt

    Pages 259-292

11. Carbon

    • Brian E. Mann

    Pages 293-303

12. Silicon, Germanium, Tin, and Lead

    • John D. Kennedy, W. McFarlane

    Pages 305-333

13. Nitrogen

    • Joan Mason

    Pages 335-367

14. Phosphorus to Bismuth

    • Keith R. Dixon

    Pages 369-402

15. Oxygen

    • W. McFarlane, H. C. E. McFarlane

    Pages 403-416

16. Sulfur, Selenium, and Tellurium

    • H. C. E. McFarlane, W. McFarlane

    Pages 417-435

17. Fluorine

    • Cynthia J. Jameson

    Pages 437-446

18. The Quadrupolar Halides

    • J. W. Akitt

    Pages 447-461

19. The Noble Gases

    • Cynthia J. Jameson

    Pages 463-477

20. Early Transition Metals, Lanthanides and Actinides

    • Dieter Rehder

    Pages 479-519

With the power and range of modern pulse spectrometers the compass of NMR spec­ troscopy is now very large for a single book-but we have undertaken this. Our book covers the Periodic Table as multinuclear spectrometers do, and introductory chapters are devoted to the essentials of the NMR experiment and its products. Primary products are chemical shifts (including anisotropies), spin-spin coupling constants, and relaxation times; the ultimate product is a knowledge of content and constitution, dynamic as well as static. Our province is chemical and biochemical rather than physical or technical; only passing reference is made to metallic solids or unstable species, or to practical NMR spectroscopy. Our aim is depth as well as breadth, to explain the fundamental processes, whether of nuclear magnetic shielding, spin-spin coupling, relaxation, or the multiple pulse sequences that have allowed the development of high-resolution studies of solids, multidimensional NMR spectroscopy, techniques for sensitivity enhancement, and so on. This book therefore combines the functions of advanced textbook and reference book. For reasonably comprehensive coverage in a single volume we have sum­ marized the information in tables and charts, and included all leading references.

• Barium
• Calcium
• Magnesium
• Mangan
• Oxidation
• Strontium
• Titan
• Vanadium
• biomolecule
• chemistry
• enzyme
• enzymes
• inorganic chemistry
• nuclear magnetic resonance (NMR)
• spectroscopy

• The Open University, Milton Keynes, Buckinghamshire, England

  Joan Mason

Policies and ethics