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Analysis with Supercritical Fluids: Extraction and Chromatography

  • Book
  • © 1992

Overview

Editors:
  1. Bernd Wenclawiak

    1. Fachbereich 8, Analytische Chemie I, Universität-GH Siegen, Siegen, Germany

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Table of contents (11 chapters)

  1. Front Matter

    Pages I-XIV
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  2. SFC and SFE: An Introduction for Novices

    • Bernd Wenclawiak
    Pages 1-8

  3. Physico-chemical Principles of Supercritical Fluid Separation Processes

    • Gerhard M. Schneider
    Pages 9-31

  4. Basic Principles of Analytical Supercritical Fluid Extraction

    • Jerry W. King, John E. France
    Pages 32-60

  5. Coupled Supercritical Fluid Extraction-Capillary Gas Chromatography (SFE-GC)

    • Steven B. Hawthorne
    Pages 61-73

  6. Gradients in SFC

    • Ernst Klesper, Franz P. Schmitz
    Pages 74-99

  7. Injection Techniques in SFC

    • Tyge Greibrokk
    Pages 100-115

  8. Stationary Phases for Packed Column Supercritical Fluid Chromatography

    • Colin F. Poole, John W. Oudsema, Thomas A. Dean, Salwa K. Poole
    Pages 116-133

  9. Enantiomer Separation by Capillary Supercritical Fluid Chromatography

    • Michael Schleimer, Volker Schurig
    Pages 134-150

  10. Supercritical Fluid Chromatography/ Mass Spectrometry

    • J. David Pinkston
    Pages 151-177

  11. Supercritical Fluid Chromatography with FT-IR Detection

    • Larry T. Taylor, Elizabeth M. Calvey
    Pages 178-189

  12. Supersonic Jet Spectroscopy with Supercritical Fluids

    • Chung Hang Sin, Steven R. Goates, Milton L. Lee, David M. Lubman
    Pages 190-202

  13. Back Matter

    Pages 203-213
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Keywords

About this book

The use of supercritical fluids in analytical chemistry is still grow­ ing. More and more analysts are discovering the favorable advan­ tages for a number of applications. Especially supercritical fluid extraction (SFE) has attracted a lot of interest in recent years due to its simplicity. Supercritical fluid chromatography (SFC) has become better established and the development of this technique has been accelerated by the many applications with capillary col­ umns which have been published in the literature. At first SFC equipment was based on instruments commonly used for liquid chromatography, and the first commercial in­ struments were derived from this technology. However, capillary columns can be much more easily interfaced to gas chromatogra­ phy equipment especially to the detectors commonly used for Oc. Many stationary phases both for packed micro columns and capillary columns have been designed for SFC purposes extending this technology to LC and OC. The most common fluid applied in SFC and SFE is carbon dioxide. The advantages of supercritical CO , such as having dif­ 2 fusivity like a gas and solvating power depending on temperature and pressure, are also valid for other fluids and modified fluids. Both properties are valuable for sample extraction and extraction selectivity.

Editors and Affiliations

  • Fachbereich 8, Analytische Chemie I, Universität-GH Siegen, Siegen, Germany

    Bernd Wenclawiak

Bibliographic Information

  • Book Title: Analysis with Supercritical Fluids: Extraction and Chromatography

  • Editors: Bernd Wenclawiak

  • DOI: https://doi.org/10.1007/978-3-642-77474-4

  • Publisher: Springer Berlin, Heidelberg

  • eBook Packages: Springer Book Archive

  • Copyright Information: Springer-Verlag Berlin Heidelberg 1992

  • Softcover ISBN: 978-3-642-77476-8Published: 21 December 2011

  • eBook ISBN: 978-3-642-77474-4Published: 06 December 2012

  • Edition Number: 1

  • Number of Pages: XIV, 214

  • Topics: Analytical Chemistry, Food Science, Biochemistry, general

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