Phosphorus-31 NMR Spectroscopy

A Concise Introduction for the Synthetic Organic and Organometallic Chemist

Authors: Kühl, Olaf

  • Good and quick overview of the topic
  • Written for the Synthetic Chemist keeping theoretical considerations to a minimum
  • Particularly well suited for the identification and prediction of new compounds
  • Explains the structure-spectra relationship
  • Unique coverage of its subject
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About this Textbook

Nuclear Magnetic Resonance is a powerful tool, especially for the identification of 1 13 hitherto unknown organic compounds. H- and C-NMR spectroscopy is known and applied by virtually every synthetically working Organic Chemist. Con- quently, the factors governing the differences in chemical shift values, based on chemical environment, bonding, temperature, solvent, pH, etc. , are well understood, and specialty methods developed for almost every conceivable structural challenge. Proton and carbon NMR spectroscopy is part of most bachelors degree courses, with advanced methods integrated into masters degree and other graduate courses. In view of this universal knowledge about proton and carbon NMR spectr- copy within the chemical community, it is remarkable that heteronuclear NMR is still looked upon as something of a curiosity. Admittedly, most organic compounds contain only nitrogen, oxygen, and sulfur atoms, as well as the obligatory hydrogen and carbon atoms, elements that have an unfavourable isotope distribution when it comes to NMR spectroscopy. Each of these three elements has a dominant isotope: 14 16 32 16 32 N (99. 63% natural abundance), O (99. 76%), and S (95. 02%), with O, S, and 34 14 S (4. 21%) NMR silent. N has a nuclear moment I = 1 and a sizeable quadrupolar moment that makes the NMR signals usually very broad and dif cult to analyse.

Table of contents (7 chapters)

Buy this book

eBook $59.99
price for USA (gross)
  • ISBN 978-3-540-79118-8
  • Digitally watermarked, DRM-free
  • Included format: PDF
  • ebooks can be used on all reading devices
  • Immediate eBook download after purchase
Softcover $79.95
price for USA
  • ISBN 978-3-540-79117-1
  • Free shipping for individuals worldwide
  • Usually dispatched within 3 to 5 business days.
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Bibliographic Information

Bibliographic Information
Book Title
Phosphorus-31 NMR Spectroscopy
Book Subtitle
A Concise Introduction for the Synthetic Organic and Organometallic Chemist
Authors
Copyright
2008
Publisher
Springer-Verlag Berlin Heidelberg
Copyright Holder
Springer-Verlag Berlin Heidelberg
eBook ISBN
978-3-540-79118-8
DOI
10.1007/978-3-540-79118-8
Softcover ISBN
978-3-540-79117-1
Edition Number
1
Number of Pages
XIV, 132
Number of Illustrations and Tables
145 b/w illustrations
Topics