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Materials | Soft-Matter Characterization

Soft-Matter Characterization

Borsali, Redouane, Pecora, Robert (Eds.)

2008, LXXII, 1452 p. In 2 volumes, not available separately.

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  • Provides comprehensive coverage of the entire field
  • Presents a comprehensive treatment of the major techniques for studying soft matter at the nanoscale level
  • Accessible to an interdisciplinary audience

Progress in basic soft matter research is driven largely by the experimental techniques available. Much of the work is concerned with understanding them at the microscopic level, especially at the nanometer length scales that give soft matter studies a wide overlap with nanotechnology.

This 2 volume reference work, split into 4 parts, presents detailed discussions of many of the major techniques commonly used as well as some of those in current development for studying and manipulating soft matter. The articles are intended to be accessible to the interdisciplinary audience (at the graduate student level and above) that is or will be engaged in soft matter studies or those in other disciplines who wish to view some of the research methods in this fascinating field.

Part 1 contains articles with a largely (but, in most cases, not exclusively) theoretical content and/or that cover material relevant to more than one of the techniques covered in subsequent volumes. It includes an introductory chapter on some of the time and space-time correlation functions that are extensively employed in other articles in the series, a comprehensive treatment of integrated intensity (static) light scattering from macromolecular solutions, as well as articles on small angle scattering from micelles and scattering from brush copolymers. A chapter on block copolymers reviews the theory (random phase approximation) of these systems, and surveys experiments on them (including static and dynamic light scattering, small-angle x-ray and neutron scattering as well as neutron spin echo (NSE) experiments). This chapter describes block copolymer behavior in the "disordered phase" and also their self-organization. The volume concludes with a review of the theory and computer simulations of polyelectrolyte solutions.

Part 2 contains material on dynamic light scattering, light scattering in shear fields and the related techniques of fluorescence recovery after photo bleaching (also called fluorescence photo bleaching recovery to avoid the unappealing acronym of the usual name), fluorescence fluctuation spectroscopy, and forced Rayleigh scattering. Volume 11 concludes with an extensive treatment of light scattering from dispersions of polysaccharides.

Part 3 presents articles devoted to the use of x-rays and neutrons to study soft matter systems. It contains survey articles on both neutron and x-ray methods and more detailed articles on the study of specific systems- gels, melts, surfaces, polyelectrolytes, proteins, nucleic acids, block copolymers. It includes an article on the emerging x-ray photon correlation technique, the x-ray analogue to dynamic light scattering (photon correlation spectroscopy).

Part 4 describes direct imaging techniques and methods for manipulating soft matter systems. It includes discussions of electron microscopy techniques, atomic force microscopy, single molecule microscopy, optical tweezers (with applications to the study of DNA, myosin motors, etc.), visualizing molecules at interfaces, advances in high contrast optical microscopy (with applications to imaging giant vesicles and motile cells), and methods for synthesizing and atomic force microscopy imaging of novel highly branched polymers..

Soft matter research is, like most modern scientific work, an international endeavor. This is reflected by the contributions to these volumes by leaders in the field from laboratories in nine different counties. An important contribution to the international flavor of the field comes, in particular, from x-ray and neutron experiments that commonly involve the use of a few large facilities that are multinational in their staff and user base.

Content Level » Research

Keywords » Complex Liquids - Nanotechnology - Optical Grating Techniques - Scattering Techniques - Soft Condensed Matter - Soft-Matter Reference

Related subjects » Biophysics & Biological Physics - Characterization & Evaluation of Materials - Materials - Nanotechnology - Polymer Science

Table of contents / Preface / Sample pages 


1. Basic Concepts – Scattering and Time Correlation Functions (R. Pecora)
2. Total Intensity Light Scattering from Solutions Macromolecules (G.C. Berry)
3. Disordered Phase and Self-Organization of Block Copolymer Systems (C. Giacomelli and R. Borsali)
4. Small-Angle Scattering from Surfactants and Block Copolymer Micelles (J.S. Pedersen)
5. Brush-Like Polymers (Y. Nakamaru and T. Norisuye)
6. Polyelectrolytes-Theory and Simulations (C. Holm)
7. Dynamic Light Scattering (B. Chu)
8. Light Scattering from Multicomponent Polymer Systems in Shear Fields: Real-time, In Situ Studies of Dissipative Structures in Open Nonequilibrium Systems (T. Hashimoto)
9. Light Scattering from Polysaccharides as Soft Material (W. Burchard)
10. Fluorescence Photobleaching Recovery (P.S. Russo, J. Qiu, N. Edwin, Y.W. Choi, G. J. Doucet, and D. Sohn)
11. Fluorescence Correlation Spectroscopy (E. Haustein and P. Schwille)
12. Forced Rayleigh Scattering – Principles and Application (Self Diffusion of Spherical Nanoparticles and Copolymer Micelles) (W. Schärtl)


13. Small-Angle Neutron Scattering and Applications in Soft Condensed Matter (I. Grillo)
14. Small Angle Neutron Scattering on Gels (M. Shibayama)
15. Complex Melts under Extreme Conditions: From Liquid Crystal to Polymers (L. Noirez)
16. In Situ Investigation of Adsorbed Amphiphilic Block Copolymers by Ellipsometry and Neutron Reflectometry (R. Toomey and M. Tirrell)
17. Synchroton Small-Angle X-Ray Scattering (T. Narayanan)
18. X-Ray Photon Correlation Spectroscopy (XPCS) (G. Grübel, A. Madsen, and A. Robert)
19. Analysis of Polyelectrolytes by Small-Angle X-Ray Scattering (M. Ballauff)
20. Small-Angle Scattering of Block Copolymers (I. Hamley and V. Castelletto)
21. Structural Studies of Proteins and Nucleic Acids in Solution Using Small-Angle X-Ray Scattering (SAXS) (R. Das and S. Doniach)
22. Transmission Electron Microscopy Imaging of Block Copolymer Aggregates in Solutions (N. Duxin and A. Eisenberg)
23. Single-Molecule Studies of DNA (J.P. Rickgauer and D.E. Smith)
24. Single Molecule Microscopy (Y. Ishii, J. Kozuka, S. Esaki and T. Yanagida)
25. Visualising Properties of Polymers at Interfaces (G. Reiter)
26. Optical Microscopy of Fluctuating Giant Vesicles and Motile Cells (H.G. Döbereiner)
27. Highly-Branched Polymers: From Comb to Dendritic Architectures (P. Viville, M. Schappacher, R. Lazarroni, and A. Deffieux)
28. AFM Imaging in Physiological Environment: From Biomolecules to Living Cells (T. Cohen-Bouhacina and A. Maali)

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