Applications of the Newer Techniques of Analysis

1. Front Matter

   Pages i-viii

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2. Raman Spectroscopy for the Study of Nematic Liquid Crystals

   • Bernard J. Bulkin

   Pages 1-12

3. Recent Developments in Arc Emission Spectroscopy: Introductory Remarks

   • Ramon M. Barnes

   Pages 13-21

4. Advances in the Static-Argon, Dc-Arc Spectrochemical Source

   • W. A. Gordon, K. M. Hambidge, M. L. Franklin

   Pages 23-43

5. The Use of Calculated X-Ray Powder Patterns in the Interpretation of Quantitative Analysis

   • C. Clark, D. K. Smith, G. G. Johnson Jr.

   Pages 45-60

6. Silica Analysis of Industrial Hygiene Samples by X-Ray Diffraction: Interim Report

   • D. T. Donovan, J. W. Knauber, F. H. VonderHeiden

   Pages 61-79

7. Applications of X-Ray Diffraction in Occupational Health Studies

   • Charles M. Nenadic, John V. Crable

   Pages 81-101

8. Determination of Composition of Solid Solutions Using X-Ray Diffraction Techniques

   • Paul Cherin

   Pages 103-122

9. NMR of Less-Sensitive Spin — 1/2 Nuclei

   • Robert R. Sharp

   Pages 123-153

10. NMR of Solutions of Alkali Metal Ions and Other Nuclei with Spin Greater Than 1/2

    • Anthony L. Van Geet

    Pages 155-163

11. Liquid Chromatography of Metal-Organic Complexes

    • Hans Veening

    Pages 165-178

12. Liquid Chromatography: Its Use as an Analytical Tool in the Pharmaceutical Laboratory

    • O. N. Hinsvark, W. Zazulak, P. Kraus, J. M. Marinello

    Pages 179-192

13. Column Packings and Efficiency in High Pressure Liquid Chromatography

    • Karl J. Bombaugh

    Pages 193-210

14. Quantitative Thin Layer Chromatography of Amino Acids

    • Helen K. Berry

    Pages 211-222

15. Single-Column Analysis of Amino Acids

    • J. Robert Benson

    Pages 223-236

16. Factors Affecting the Reproducibility in Pyrolysis Gas Chromatography (PGC)

    • Clarence J. Wolf, Ram L. Levy

    Pages 237-250

17. Laser Induced Pyrolysis Gas Chromatography

    • Nicholas E. Vanderborgh

    Pages 251-272

18. Applications of Combined Gas Chromatography-Mass Spectrometry in Clinical Chemistry

    • John Roboz

    Pages 273-301

19. Applications of Mass Spectrometry in Drug Metabolism and Related Fields

    • W. J. A. Vanden

    Pages 303-343

20. Chemical Ionization Mass Spectrometry

    • David P. Beggs

    Pages 345-357

This volume presents a group of selected papers given at the November, 1972, meeting of the Eastern Analytical Symposium. As has always been the intent of the series, "Progress in Analytical Chemistry," the papers are written by authorities who are also active workers in their fields. Included are applications of Raman Spectroscopy, X-Ray Diffraction, Emission Spectroscopy, Nu­ clear Magnetic Resonance, Liquid Chromatography, Thin-Layer Chromatography, Pyrolysis Gas Chromatography, Mass Spectrometry, Gas Chromatography and the powerful marriage of the last two. In modern analysis there is a constant search for applications of existing instrumentation in new ways to produce results hitherto unobtainable. In every case both the versatility of the researcher and the flexibility of the method used are amply illustrated. Thanks are due to the authors of the papers for their efforts in coping with the many problems of producing a manuscript in finished form enabling rapid publication. Ivor L. Simmons Galen W. Ewing v CONTENTS Raman Spectroscopy for the Study of Nematic Liquid Crystals . . . . . . 1 Bernard J. Bulkin Recent Developments in Arc Emission Spectroscopy: Introductory Remarks . . . . . . . . . . 13 Ramon M. Barnes Advances in the Static-Argon, DC-ARC Spectrochemical Source . . • . . 23 W. A. Gordon, K. M. Hambidge, and M. L. Franklin The Use of Calculated X-ray Powder Patterns in the Interpretation of Quantitative Analysis 45 C. Clark, D. K. Smith, and G. G. Johnson, Jr.

• analytical chemistry
• chromatography
• spectroscopy

• M&T Chemicals, Inc., Rahway, USA

  Ivor L. Simmons

• Seton Hall University, South Orange, USA

  Galen W. Ewing

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