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In-situ Small-Angle X-ray Scattering Investigation of Transient Nanostructure of Multi-phase Polymer Materials Under Mechanical Deformation

  • Book
  • © 2013

Overview

Authors:
  1. Ahmad Zeinolebadi

    1. Chemistry, University of Hamburg, Current: Polymer Consult Buchner GmbH, Institute of Technical & Macromolecular, Hamburg, Germany

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  • Nominated by the University of Hamburg (Germany) as an outstanding PhD thesis
  • Answers a central question in polymer materials research: "Why don't prepared composites show less fatigue than the pure plastics?"
  • Applies a simultaneous analysis of mechanical testing and X-Ray scattering at DESY in Hamburg
  • Includes supplementary material: sn.pub/extras

Part of the book series: Springer Theses (Springer Theses)

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Table of contents (7 chapters)

  1. Front Matter

    Pages i-xvi
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  2. Introduction

    • Ahmad Zeinolebadi
    Pages 1-22

  3. Experimental Part

    • Ahmad Zeinolebadi
    Pages 23-27

  4. Data Evaluation

    • Ahmad Zeinolebadi
    Pages 29-38

  5. Thermoplastic Polyurethane Elastomers Under Uniaxial Deformation

    • Ahmad Zeinolebadi
    Pages 39-56

  6. Polypropylene/Montmorillonite Nanocomposites: Continuous Stretching and Load-Cycling

    • Ahmad Zeinolebadi
    Pages 57-81

  7. HDPE/PA Microfibrillar Composites Under Load-Cycling

    • Ahmad Zeinolebadi
    Pages 83-98

  8. Summary and Future Works

    • Ahmad Zeinolebadi
    Pages 99-102

  9. Back Matter

    Pages 103-106
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Keywords

About this book

The results in this dissertation set the ground to answer a fundamental question in data-driven polymer material science: "Why don't prepared composites show less fatigue than the pure plastics?" A simultaneous analysis of mechanical testing and small angle X-Ray scattering from the DESY source in Hamburg has been applied to approach this question, which is also central to the European research project "Nanotough", and the results are clearly presented in this book. The evolution of the materials structure is visualized and quantitatively analyzed from exhaustive sequences of scattering images. Three different classes of polymer composites are presented as typical and illustrative examples. The obtained results illustrate that the interactions of their components can cause unpredictable structural effects, ultimaltely leading to a weakening of the material, where a reinforcement was expected.

Authors and Affiliations

  • Chemistry, University of Hamburg, Current: Polymer Consult Buchner GmbH, Institute of Technical & Macromolecular, Hamburg, Germany

    Ahmad Zeinolebadi

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