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Chemistry - Catalysis | MWW-Type Titanosilicate - Synthesis, Structural Modification and Catalytic Applications to Green

MWW-Type Titanosilicate

Synthesis, Structural Modification and Catalytic Applications to Green Oxidations

Wu, P., Xu, H., Xu, L., Liu, Y., He, M.

2013, VIII, 125 p. 79 illus., 25 illus. in color.

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  • Provides a complete overview of the Ti-MWW catalyst
  • Describes detailed synthesis methods for preparing Ti-MWW that differ from conventional techniques
  • Shows the special role of Ti-MWW titanosilicate in structure change, which improves its catalytic performance
  • Covers useful reactions catalyzed by Ti-MWW zeolite

This book provides a comprehensive review of a new generation of selective oxidation titanosilicate catalysts with the MWW topology (Ti-MWW) based on the research achievements of the past 12 years. It gives an overview of the synthesis, structure modification and catalytic properties of Ti-MWW. Ti-MWW can readily be prepared by means of direct hydrothermal synthesis with crystallization-supporting agents, using dual-structure-directing agents and a dry-gel conversion technique. It also can be post-synthesized through unique reversible structure transformation and liquid-phase isomorphous substitution. The structural conversion of Ti-MWW into the materials usable for processing large molecules is summarized. Taking advantage of the structure diversity of the lamellar precursor of Ti-MWW, it can be fully or partially delaminated, and undergo interlayer silylation to obtain a novel structure with larger porosity. In the selective oxidation (alkene epoxidation and ketone/aldehyde ammoximation) with hydrogen peroxide or organic peroxide as an oxidant, the unique catalytic properties of Ti-MWW are described in comparison to conventional titanosilicates such as TS-1 and Ti-Beta.

Content Level » Research

Keywords » Aldehyde Ammoximation - Alkene Epoxidation - Heterogeneous Catalysis - Hydrogen Peroxide - Ketone Ammoximation - Selective Oxidation - TS-1 Zeolite - Ti-MWW Zeolite - Titanosilicate Zeolite - Zeolite Catalysts

Related subjects » Catalysis - Environmental Chemistry - Industrial Chemistry and Chemical Engineering - Physical Chemistry

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