Advanced Magnetic Resonance Techniques in Systems of High Molecular Complexity

1. Front Matter

   Pages i-x

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2. Spatial Localization in NMR

   • A. J. Shaka, Ray Freeman

   Pages 1-19

3. Homonuclear Hartmann-Hahn Magnetization Transfer: New One- and Two-Dimensional NMR Methods for Structure Determination and Spectral Assignment

   • A. Bax, D. G. Davies

   Pages 21-48

4. Simplification of 2D Spectra by (a) Topology-Selective Multiple-Quantum Filtration or (b) by Bilinear Mixing

   • M. H. Levitt, C. Radloff, R. R. Ernst

   Pages 49-52

5. 17O NMR as a Probe to Study Hydration and Hydrogen Bonding of Amino Acids and Polypeptides

   • A. Spisni, E. D. Gotsis, E. Ponnusamy, D. Fiat

   Pages 53-60

6. Indirect, Negative Heteronuclear Overhauser Effect Detected in a Steady-State, Selective 13C-{1H} NOE Experiment at Natural Abundance

   • K. E. Kövér, G. Batta

   Pages 61-67

7. Determination of Zero- and Double-Quantum Relaxation Transition Probabilities by Multiple-Selective Irradiation Methods

   • G. Valensin, G. Sabatini, E. Tiezzi

   Pages 69-76

8. The Role of Conformation and Conformational Dynamics in Biological Information Transfer

   • W. A. Gibbons, P. Mascagni, N. Zhou, A. E. Aulabaugh, A. Prugnola, M. Kuo et al.

   Pages 77-88

9. Structure and Dynamics Studied Via Two-Dimensional NMR. Illustrations with DNA Fragments

   • Thomas L. James, Michelle S. Broido, Nadege Jamin, Gregory B. Young, Gerald Zon

   Pages 89-108

10. Selective 1H NMR Relaxation Delineation of Receptor Binding Equilibria

    • E. Gaggelli, A. Lepri, N. Marchettini, S. Ulgiati

    Pages 109-117

11. Nuclear Spin Relaxation Study of Weak Molecular Interactions in Benzene Solutions of Quinuclidine

    • A. Maliniak, J. Kowalewski

    Pages 119-123

12. Proton NMR Studies of the Active Centre of ACTH

    • F. Toma, V. Dive, M. Löw, L. Kisfaludy

    Pages 125-133

13. 13C and 1H NMR Characterization of a Na+ClO4 - Complex of a New Lipophilic Cage Ligand

    • P. L. Anelli, T. Beringhelli, H. Molinari, F. Montanari, S. Quici

    Pages 135-139

14. B and Z Forms of a Modified d(C-G) Sequence in Solution

    • L. P. M. Orbons, G. A. van der Marel, J. H. van Boom, C. Altona

    Pages 141-147

15. NMR Study of a Tridecanucleotide Containing a No-Base Residue

    • S. Pochet, T. Huynh-Dinh, J. M. Neumann, S. Tran-Dinh, J. Igolen

    Pages 149-155

16. Dynamic Nuclear Magnetic Resonance of Caprimidyl Sulfate

    • G. Gurato, G. Nadali, M. F. Coletta

    Pages 157-163

17. Solvent Proton Nuclear Magnetic Relaxation Dispersion (NMRD) in Solutions of Paramagnetic Macromolecules

    • Ivano Bertini, Fabrizio Briganti, Claudio Luchinat

    Pages 165-195

18. Nuclear Spin Relaxation in Paramagnetic Nickel (II) Complexes

    • J. Kowalewski, N. Benetis, T. Larsson, P.-O. Westlund, H. Wennerström

    Pages 197-211

19. Multipulse Dynamic Nuclear Magnetic Resonance Theory and Applications to Liquid Crystal Polymers

    • K. Müller, P. Meier, G. Kothe

    Pages 213-231

20. Deuterium Spin Relaxation and Molecular Motion in Liquid Crystals

    • R. L. Vold, R. R. Vold, J. F. Martin, B. C. Nishida, L. S. Selwyn

    Pages 233-251

The second volume of the series on inorganic biochemistry and bio­ physics is singularly devoted to magnetic resonance on systems of high molecular complexity. Recently, there have been important advances in magnetic resonance studies of polymers; these advances touch on all aspects of magnetic resonance, both theoretical and applied. Particular emphasis is placed here on multipulse experiments. We believe such an report will be of considerable interest to the readers of our series owing to the importance of magnetic resonance techniques in the investigation of biopolymers. Ivano Bertini Harry Gray Series Editors Preface This book is a record of the Proceedings of the International Symposium on "Advanced Magnetic Resonance Techniques in Systems of High Molecular Complexity", which was held in Siena between 15 and 18 May 1985. The idea of the meeting is due to Proff. N.M. Atherton, G. Giacometti and E. Tiezzi with the aim of honouring the scientific personality of Prof. S.I. Weissman. The meeting has been organized with the assistance of a National Committee formed by R. Basosi, I. Bertini, P. Bucci, C. Corvaia, A. Gamba, G. Martini, G.F. Pedulli, P.A. Temussi, and C.A. Veracini. The invited lecturers responded enthusiastically and a comprehensive picture of the theoretical and practical aspects of magnetic resonance could be therefore provided. The book contains all the plenary lectures delivered during the meeting and also a wide selection among the huge amount of contributions collected by the organizers.

• Amino acid
• DNA
• Peptide
• electron spin
• electron spin echo
• magnetic resonance
• spectroscopy

• Department of Chemistry, University of Siena, Siena, Italy

  Neri Niccolai, Gianni Valensin

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