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Studies on Porous Monolithic Materials Prepared via Sol–Gel Processes

  • Book
  • © 2013

Overview

Authors:
  1. George Hasegawa

    1. , Graduate School of Engineering, Kyoto University, Kyoto, Japan

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  • Was named best-in-department thesis (Chemistry, 2012) from the Graduate School of Science, Kyoto University
  • Presents state-of-the-art porous monoliths based on various chemical compositions (organic, inorganic, and organic–inorganic hybrid materials) fabricated via the sol–gel method accompanied by phase separation
  • Includes many electron micrographs, helping general readers to understand the pore structures of the materials

Part of the book series: Springer Theses (Springer Theses)

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Table of contents (14 chapters)

  1. Front Matter

    Pages i-xv
    Download chapter PDF

  2. General Introduction

    • George Hasegawa
    Pages 1-11

  3. Pore Formation in Poly(divinylbenzene) Networks Derived from Organotellurium-Mediated Living Radical Polymerization

    • George Hasegawa
    Pages 13-32

  4. Extension of Living Radical Polymerization Accompanied by Phase Separation to Methacrylate- and Acrylamide-based Polymer Monoliths

    • George Hasegawa
    Pages 33-45

  5. Novel Monolithic Capillary Column with Well-Defined Macropores Based on Poly(styrene-co-divinylbenzene)

    • George Hasegawa
    Pages 47-60

  6. Fabrication of Activated Carbon Monoliths with Well-Defined Macropores Derived from Sulfonated Poly(divinylbenzene) Networks

    • George Hasegawa
    Pages 61-78

  7. Monolithic Electrode for Electric Double-Layer Capacitors Based on Macro/Meso/Microporous S-Containing Activated Carbon with High Surface Area

    • George Hasegawa
    Pages 79-89

  8. Facile Preparation of Transparent Monolithic TiO2 Gels Utilizing Chelating Ligand and Mineral Salts

    • George Hasegawa
    Pages 91-105

  9. Novel and Facile Preparation of Hierarchically Porous TiO2 Monoliths

    • George Hasegawa
    Pages 107-119

  10. Application of Hierarchically Porous Titania Monoliths to Chromatographic Separation Media

    • George Hasegawa
    Pages 121-134

  11. Arylene-Bridged Polysilsesquioxane Monoliths with Multi-Scale Porous Structure Prepared via Sol–Gel Process Followed by Hydrothermal Treatment

    • George Hasegawa
    Pages 135-145

  12. Fabrication of Macroporous SiC and SiC/C Monoliths from Arylene-Bridged Polysilsesquioxanes via Carbothermal Reduction

    • George Hasegawa
    Pages 147-162

  13. Hierarchically Porous Carbon Monoliths with High Surface Area from Arylene-Bridged Polysilsesquioxanes Without Thermal Activation Process

    • George Hasegawa
    Pages 163-179

  14. Facile Preparation of Monolithic LiFePO4/Carbon Composites with Well-Defined Macropores for Li-ion Battery

    • George Hasegawa
    Pages 181-202

  15. General Summary

    • George Hasegawa
    Pages 203-207
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Keywords

About this book

This thesis focuses on porous monolithic materials that are not in the forms of particles, fibers, or films. In particular, the synthetic strategy of porous monolithic materials via the sol–gel method accompanied by phase separation, which is characterized as the non-templating method for tailoring well-defined macropores, is described from the basics to actual synthesis. Porous materials are attracting more and more attention in various fields such as electronics, energy storage, catalysis, sensing, adsorbents, biomedical science, and separation science. To date, many efforts have been made to synthesize porous materials in various chemical compositions—organics, inorganics including metals, glasses and ceramics, and organic-inorganic hybrids. Also demonstrated in this thesis are the potential applications of synthesized porous monolithic materials to separation media as well as to electrodes for electric double-layer capacitors (EDLCs) and Li-ion batteries (LIBs). This work is ideal for graduate students in materials science and is also useful to engineers or scientists seeking basic knowledge of porous monolithic materials.

Authors and Affiliations

  • , Graduate School of Engineering, Kyoto University, Kyoto, Japan

    George Hasegawa

About the author

Dr. George Hasegawa
Department of Energy and Hydrocarbon Chemistry,
Graduate School of Engineering, Kyoto University

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